Mass Spec Analytical Ltd

home Products Services contact
 
   

Up
Analysis
Consultancy

Mass Spec Analytical Ltd - Logo

Forensic Scientist / Analytical Chemist :

Mass Spec Analytical Ltd.
Building 20F
Golf Course Lane
PO Box 77
Filton
Bristol BS99 7AR
UK

Registered in England
  No. 3000979

Copyright © 2007
Mass Spec Analytical Ltd.
All Rights Reserved

 

Mass Spec Analytical - Logo

Products & Services

Mass Spec Analytical Ltd. (MSA) has a specialised team of scientists dedicated to the analysis of a wide range of exhibits for traces of drugs and explosives.

Services:-

bulletWide range of exhibits are rapidly tested for drugs or explosives traces; including mobile phones, vehicles, clothing, premises, documents & personal items
bulletBanknotes tested for traces of drugs
bulletMatching of drug batches using IRMS technology
bulletThousands of analysis tasks completed for Police Forces, HM Customs & Defence Teams
bulletExpert Witness evidence presented in court
bulletSimple and effective sample collection techniques
bulletRemote Sampling Kits supplied for the collection of dust samples from vehicles & premises
bulletCall out our mobile tandem mass spectrometer Scentinel® providing instant results
bulletResearch & Development contracts in trace detection performed over a number of years
bulletAlcohol in Blood and Urine Analysis
bulletGCMS Analysis - compound identification and concentration

Products

bulletSpecialist sample introduction devices designed & supplied
bulletMobile tandem mass spectrometer Scentinel®
bulletBoarding Pass Analyser for the detection of explosives on aircraft boarding passes
bulletEquipment can be supplied for detection of drugs & explosives traces at ports and border crossings
bulletRemote Sampling Kits supplied for the collection of dust samples from vehicles & premises

Fill in request or contact us for further details

Recommendations for Handling Exhibits for Trace Analysis

General Points

Be Aware

Locard's Principle states that "every contact leaves a trace", and therefore every time an exhibit is handled there is the possibility that two-way transfer (cross contamination) may occur. It is not possible to identify how any particular trace may have arisen, or how long it has been present. The implication for law enforcement agencies is that it is likely to be suggested in court that they themselves are the source of any material found.

Avoid Contact

The safest way to ensure the forensic integrity of an exhibit is not to touch it.

Wear Gloves

If it is necessary to touch an exhibit, precautions need to be taken to minimise the possibility of transferring material. This is a two way process; it is important to minimise the contamination of the exhibit from the officer involved, and it is also important to minimise the contamination of the officer from the exhibit. If an officer becomes contaminated, it is possible that material will be transferred to items subsequently touched.

Oversuits and shoes can also help minimise transfer.

Ensure Cleanliness

It is one thing to say that gloves were worn; but another to prove it. Retaining gloves (or oversuits) as exhibits helps. These would then be available to the defence if required (although analysis after use is of questionable value since it is not possible to say whether they were contaminated to start with or whether they became contaminated through contact with the exhibit). Another way of helping to ensure that particular individuals were not a source of contamination is to ask them to handle a clean piece of paper prior to handling the exhibit. This paper can then be submitted as an exhibit to demonstrate cleanliness.

Change Gloves

Remember that the purpose of wearing gloves is to isolate a particular item from the person. The same gloves should therefore not be used to handle another item.

Double Bag

Exhibits should be double bagged, preferably in plastic bags, with both sealed. Note that the use of plastic bags is not the preferred choice for certain other types of forensic analysis. If in doubt consult MSA or the FSS hotline. The use of two bags further distances an exhibit from other potential sources of contamination. It could also be argued that certain compounds are capable of passing through plastic, and thus, double bagging reduces the possibility of this happening.

Do Not Mix Bulk and Trace Exhibits

If both bulk and trace exhibits are involved, it is our recommendation that trace exhibits should be handled before the bulk drugs. No-one will argue that a bulk drug was significantly altered by a trace, but the converse could certainly be argued. If at all possible, bulk drugs and exhibits to be analysed for traces should be handled by different individuals.

Preserve Chain of Evidence

This is crucially important, as for any other type of exhibit. Additionally, cash exhibits have obvious security problems. Our policy is that cash exhibits are either under seal or under video surveillance at all times.

Supply Information

Inform the laboratory of any other information which may assist in interpretation. This may include circumstances of seizure and other background intelligence. Since MSA perform “target compound analysis” it is imperative that we are informed if less common drugs are suspected, otherwise we will not look for them! Information such as the size of the total seizure, or any special requests (drugs, fingerprints, DNA, intact wrappings) would be beneficial. We routinely analyse approximately one third of the number of banknotes in an exhibit. If the exhibit is a proportion of a larger seizure, then we need to analyse a greater proportion of the exhibit in order to be able to draw significant conclusions.

Time

Exhibits for trace analysis should be submitted to the laboratory as soon as is possible (within weeks rather than months). This is because drugs traces, in particular heroin and cannabis, degrade rapidly over time, and this degradation is exacerbated by increased temperatures. If exhibits need to be stored for a period of time prior to submission, we would recommend that they are stored securely at low temperatures and away from other sources of drug contamination.

Banknotes

When making cash seizures, it is important to follow procedures to reduce cross contamination which would reduce the evidential value.

1)An inert covering should be placed on all surfaces with which the money comes into contact (foil is suitable). This is to prevent the money from coming into contact with surfaces that may be contaminated with drugs, for example, the custody desk at a Police Station, surfaces in a suspect's premises, etc. Foil is cheap and impervious to drugs. Once the exhibit has been examined, the foil should be wrapped around the money before it is bagged up. This is because the foil prevents drugs from "falling off" the banknotes and leaching out of the bag, and also prevents drugs from leaching into the bag.

2)Gloves should be worn when handling exhibits (not just cash, but any exhibits), and handling should be kept to a minimum to reduce the possible re-distribution of drugs particles. To this end, it is preferable if the cash is uncounted (although we realise that this is not always possible).

3)Weighing rather than counting can help give some indication as to whether part of an exhibit has been removed, but if counting is necessary, there are a number of steps to reduce cross contamination. First, if counting by hand, gloves should be worn, and a paper swab of the gloves taken before any handling takes place. At the same time, a piece of blank paper should also be taken, in order to show the paper is clean. Both of these control samples should be placed in bags and submitted for analysis. The gloves should also be bagged and submitted for analysis after counting to show any contamination on the gloves. Low levels of contamination on the gloves are often found and are consistent with contact with the banknotes. Counting machines can also be used to count the banknotes, but if this is the case, the counting machines should be submitted for analysis, and it would be advantageous if blank pieces of paper were run through the machine before counting, and submitted for analysis, to demonstrate any contamination of the counting machine prior to counting.

Mobile Telephones

1)Many of the above points also apply to mobile telephones. Mobile telephones can provide powerful evidence of involvement in drug-related activities, and MSA is currently building up a considerable database on the extent of contamination of mobile phones owned by the general public. Mobile telephones can also provide other useful evidence, for example, from the analysis of SIM cards, text messages etc.

2) MSA take steps to ensure that the analysis of the drug contamination on mobile telephone exhibits does not compromise later data retrieval. If mobile telephones are examined for their data records prior to bringing them to MSA then the trace evidence may be affected by cross contamination prior to delivery to MSA.

3)Gloves should be worn when handling mobile telephones, and care should be taken not to disturb any traces that may be present in or on the telephone.

Clothing

1)Clothing exhibits to be submitted for trace analysis should be handled as little as possible, in order to minimise cross contamination.

2)Care should be taken not to disturb any traces that may be present on areas of the clothing, as this would give the impression that the item had been exposed to environmental contamination, when in fact the contamination had originally been in one area, for example a pocket or turn-up.

Premises

1)When attending premises to take samples for trace analysis, gloves and an oversuit (if possible) should be worn. This is to minimise cross contamination from the clothing of individuals.

2)The oversuit should be sampled prior to entering the premises, as should the gloves (in the way already described in the Banknote section).

3)Once inside the premises, samples should be taken from relevant areas, for example, curtains, carpets, air vents, door tops, cupboards, and any areas where dust accumulates, or is inaccessible.

4)It is essential that proper notes of the sampling are made, along with diagrams and photographs (where possible).

5)It is also worth removing items from the premises for trace analysis, for example, remote controls, ashtrays, mirrors, papers and any paraphernalia, as well as swabs from the TV screen, surfaces, microwave etc.

6)Once again it is important to minimise cross contamination of exhibits, and so it is useful to try and ensure that officers attending have not come directly from the scene of a large bulk seizure, or from a 'crack-den', for example.

7)Once the sampling is finished, the gloves and oversuits should be bagged up, and made available to the defence for analysis.

Motor Vehicles

1)A similar approach to that described for premises is used for the sampling of motor vehicles.

2)The areas of the vehicle to take samples from are: the seats, boot, dashboard, steering wheel, gearstick and glove compartment. These samples are best taken using lint brushes (for the seats and the boot), and cotton swabs (for the other areas).

Counting Machines

1)Counting machines can be analysed for traces of drugs. The counting machines should be disturbed as little as possible in order to minimise redistribution of drugs particles.

2)The analysis of counting machines is undertaken by running pieces of paper (which have been shown to be clean) through the counting machine.

Vacuum Cleaners

1)The dust in vacuum cleaner bags can be analysed for traces of drugs, and this can be useful to help identify a link with drugs. The major advantages of vacuum cleaner bags are that the suspect may have taken the samples, and that the samples have been taken over a longer period of time.

2)Vacuum cleaner bags should again be disturbed as little as possible in order to minimise redistribution of drugs particles.

Hand Swabs

1)Hand swabs should be taken from a suspect as soon as possible to try and minimise the loss of drugs traces from the hands by abrasion. The swabs can be either dry swabs or moist swabs.

2)Untouched swabs, and swabs with just water on them (in the case of moist swabs) should be submitted for analysis in order to show that the swabs themselves and the water used are free from contamination.

Papers

1)Any papers (other than banknotes) can be analysed for traces of drugs in the same way as banknotes. Examples of the types of papers that can be analysed include diaries, alleged price lists, any documentation, or any papers that may have come into contact with drugs.

2)Paper exhibits should be treated in the same way as banknotes.

Other Items

1)Many other items can be analysed for the presence of drugs traces. Items can either be submitted directly for analysis, or can be sampled remotely. The samples taken can then be submitted for analysis.

2)Examples of the types of items that can be submitted for analysis are remote controls, swabs from television screens/ computer monitors, computer keyboards, carpets, weighing scales, and any other dust samples.

3)These items can either be submitted directly to the laboratory for analysis, or can be sampled using lint brushes (for carpets), cotton swabs (for dust samples, monitors, scales) or toothpicks (for keyboards and remote controls).

Document Reference : MSA4648JBL

Version No. 2

Date : 30/01/2004

 

 

Press Release June 2007 : UKAS 17025 Accreditation
Mass Spec Analytical Ltd achieves UKAS 17025 Accreditation
in areas of Drugs on Money, Packaging, Fuel Analysis and
Alcohol in Blood and Urine Analysis :
 see Press Release

Press Release April 2007 from Applied Biosystems
Mass Spec Analytical advances forensic science
through the development of innovative technology
 - see Press Release

Mass Spec Analytical
matching of packaging
material/tape published
in The Analyst journal
http://www.msaltd.co.uk/papers.htm

News Articles:
Mass Spec ensures crime doesn't pay
http://www.rsc.org/chemistryworld/News/2005/July/06070502.asp

Mass Spec Analytical - Trace Explosives Reader
Mass Spec Analytical's Forensic Scientist /
Analytical Chemist team develop a reader
which analyses 1000 tickets per hour to detect
multiple explosives simultaneously

· Handling Exhibits
· MSA Papers
· Other Papers
· How to Find MSA
· Contact us
· Want more info on a 
    product or service?

Mass Spec Analytical - Scentinel
Our Scentinel® multi-purpose
mobile Mass spectrometer
has been developed with
MDS Sciex Inc. and
J.S. Chinn P.E. Ltd.


  Home ] Company History ] Products ] [ Services ] Techniques ] Info Request ] Published Papers ] R&D ] Vacancies ] Contact Us ] Links ] RTA ]