




Forensic Scientist / Analytical Chemist :
Mass Spec Analytical Ltd.
Building 20F
Golf Course Lane
PO Box 77
Filton
Bristol BS99 7AR
UK
Registered in England
No. 3000979
Copyright © 2007
Mass Spec Analytical Ltd.
All Rights Reserved

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Products & Services
| Mass Spec Analytical Ltd. (MSA) has
a specialised team of scientists dedicated to the analysis of a wide
range of exhibits for traces of drugs and explosives. Services:-
 | Wide range of exhibits are rapidly tested for drugs or
explosives traces; including mobile phones, vehicles, clothing,
premises, documents & personal items |
 | Banknotes tested for traces of drugs |
 | Matching of drug batches using
IRMS technology |
 | Thousands of analysis tasks completed for Police Forces, HM
Customs & Defence Teams |
 | Expert Witness evidence presented in court |
 | Simple and effective sample collection techniques |
 | Remote Sampling Kits supplied for the collection of dust
samples from vehicles & premises |
 | Call out our mobile tandem mass spectrometer
Scentinel®
providing instant results |
 | Research & Development contracts in trace detection
performed over a number of years |
 | Alcohol in Blood and Urine Analysis |
 | GCMS Analysis - compound identification and concentration |
Products
 | Specialist sample introduction devices designed & supplied |
 | Mobile tandem mass spectrometer Scentinel® |
 | Boarding Pass Analyser for the detection of explosives on
aircraft boarding passes |
 | Equipment can be supplied for detection of drugs &
explosives traces at ports and border crossings |
 | Remote Sampling Kits supplied for the collection of dust
samples from vehicles & premises |
Fill
in request or contact
us for further details

Recommendations
for Handling Exhibits for Trace Analysis
General Points
Be Aware
Locard's Principle states that "every
contact leaves a trace", and therefore every time an exhibit is
handled there is the possibility that two-way transfer (cross
contamination) may occur. It is not possible to identify how any
particular trace may have arisen, or how long it has been present.
The implication for law enforcement agencies is that it is likely to
be suggested in court that they themselves are the source of any
material found.
Avoid Contact
The safest way to ensure the forensic integrity
of an exhibit is not to touch it.
Wear Gloves
If it is necessary to touch an exhibit,
precautions need to be taken to minimise the possibility of
transferring material. This is a two way process; it is important to
minimise the contamination of the exhibit from the officer involved,
and it is also important to minimise the contamination of the
officer from the exhibit. If an officer becomes contaminated, it is
possible that material will be transferred to items subsequently
touched.
Oversuits and shoes can also help minimise
transfer.
Ensure Cleanliness
It is one thing to say that gloves were worn; but
another to prove it. Retaining gloves (or oversuits) as exhibits
helps. These would then be available to the defence if required
(although analysis after use is of questionable value since it is
not possible to say whether they were contaminated to start with or
whether they became contaminated through contact with the exhibit).
Another way of helping to ensure that particular individuals were not a source
of contamination is to ask them to handle a clean piece of paper
prior to handling the exhibit. This paper can then be submitted as
an exhibit to demonstrate cleanliness.
Change Gloves
Remember that the purpose of wearing gloves is to
isolate a particular item from the person. The same gloves should
therefore not be used to handle another item.
Double Bag
Exhibits should be double bagged, preferably in
plastic bags, with both sealed. Note that the use of plastic bags is
not the preferred choice for certain other types of forensic
analysis. If in doubt consult MSA or the FSS hotline. The use of two
bags further distances an exhibit from other potential sources of
contamination. It could also be argued that certain compounds are
capable of passing through plastic, and thus, double bagging reduces
the possibility of this happening.
Do Not Mix Bulk and Trace Exhibits
If both bulk and trace exhibits are involved, it
is our recommendation that trace exhibits should be handled before
the bulk drugs. No-one will argue that a bulk drug was significantly
altered by a trace, but the converse could certainly be argued. If
at all possible, bulk drugs and exhibits to be analysed for traces
should be handled by different individuals.
Preserve Chain of Evidence
This is crucially important, as for any other
type of exhibit. Additionally, cash exhibits have obvious security
problems. Our policy is that cash exhibits are either under seal or
under video surveillance at all times.
Supply Information
Inform the laboratory of any other information
which may assist in interpretation. This may include circumstances
of seizure and other background intelligence. Since MSA perform “target
compound analysis” it is imperative that we are informed if less
common drugs are suspected, otherwise we will not look for them!
Information such as the size of the total seizure, or any special
requests (drugs, fingerprints, DNA, intact wrappings) would be
beneficial. We routinely analyse approximately one third of the
number of banknotes in an exhibit. If the exhibit is a proportion of
a larger seizure, then we need to analyse a greater proportion of
the exhibit in order to be able to draw significant conclusions.
Time
Exhibits for trace analysis should be submitted
to the laboratory as soon as is possible (within weeks rather than
months). This is because drugs traces, in particular heroin and
cannabis, degrade rapidly over time, and this degradation is
exacerbated by increased temperatures. If exhibits need to be stored
for a period of time prior to submission, we would recommend that
they are stored securely at low temperatures and away from other
sources of drug contamination.
Banknotes
When making cash seizures, it is important to
follow procedures to reduce cross contamination which would reduce
the evidential value.
1)An inert covering should be placed on all
surfaces with which the money comes into contact (foil is
suitable). This is to prevent the money from coming into contact
with surfaces that may be contaminated with drugs, for example,
the custody desk at a Police Station, surfaces in a suspect's
premises, etc. Foil is cheap and impervious to drugs. Once the
exhibit has been examined, the foil should be wrapped around the
money before it is bagged up. This is because the foil prevents
drugs from "falling off" the banknotes and leaching out
of the bag, and also prevents drugs from leaching into the bag.
2)Gloves should be worn when handling exhibits
(not just cash, but any exhibits), and handling should be kept to
a minimum to reduce the possible re-distribution of drugs
particles. To this end, it is preferable if the cash is uncounted
(although we realise that this is not always possible).
3)Weighing rather than counting can help give
some indication as to whether part of an exhibit has been removed,
but if counting is necessary, there are a number of steps to
reduce cross contamination. First, if counting by hand, gloves
should be worn, and a paper swab of the gloves taken before any
handling takes place. At the same time, a piece of blank paper
should also be taken, in order to show the paper is clean. Both of
these control samples should be placed in bags and submitted for
analysis. The gloves should also be bagged and submitted for
analysis after counting to show any contamination on the gloves.
Low levels of contamination on the gloves are often found and are
consistent with contact with the banknotes. Counting machines can
also be used to count the banknotes, but if this is the case, the
counting machines should be submitted for analysis, and it would
be advantageous if blank pieces of paper were run through the
machine before counting, and submitted for analysis, to
demonstrate any
contamination of the counting machine prior to counting.
Mobile Telephones
1)Many of the above points also apply to mobile
telephones. Mobile telephones can provide powerful evidence of
involvement in drug-related activities, and MSA is currently
building up a considerable database on the extent of contamination
of mobile phones owned by the general public. Mobile telephones can
also provide other useful evidence, for example, from the analysis of SIM
cards, text messages etc.
2) MSA take steps to ensure that the analysis of
the drug contamination on mobile telephone exhibits does not
compromise later data retrieval. If mobile telephones are examined
for their data records prior to bringing them to MSA then the trace
evidence may be affected by cross contamination prior to delivery to
MSA.
3)Gloves should be worn when handling mobile
telephones, and care should be taken not to disturb any traces that
may be present in or on the telephone.
Clothing
1)Clothing exhibits to be submitted for trace
analysis should be handled as little as possible, in order to
minimise cross contamination.
2)Care should be taken not to disturb any traces
that may be present on areas of the clothing, as this would give the
impression that the item had been exposed to environmental
contamination, when in fact the contamination had originally been in
one area, for example a pocket or turn-up.
Premises
1)When attending premises to take samples for
trace analysis, gloves and an oversuit (if possible) should be worn.
This is to minimise cross contamination from the clothing of
individuals.
2)The oversuit should be sampled prior to
entering the premises, as should the gloves (in the way already
described in the Banknote section).
3)Once inside the premises, samples should be
taken from relevant areas, for example, curtains, carpets, air
vents, door tops, cupboards, and any areas where dust accumulates,
or is inaccessible.
4)It is essential that proper notes of the
sampling are made, along with diagrams and photographs (where
possible).
5)It is also worth removing items from the
premises for trace analysis, for example, remote controls, ashtrays,
mirrors, papers and any paraphernalia, as well as swabs from the TV
screen, surfaces, microwave etc.
6)Once again it is important to minimise cross
contamination of exhibits, and so it is useful to try and ensure
that officers attending have not come directly from the scene of a
large bulk seizure, or from a 'crack-den', for example.
7)Once the sampling is finished, the gloves and
oversuits should be bagged up, and made available to the defence for
analysis.
Motor Vehicles
1)A similar approach to that described for
premises is used for the sampling of motor vehicles.
2)The areas of the vehicle to take samples from
are: the seats, boot, dashboard, steering wheel, gearstick and glove
compartment. These samples are best taken using lint brushes (for
the seats and the boot), and cotton swabs (for the other areas).
Counting Machines
1)Counting machines can be analysed for traces of
drugs. The counting machines should be disturbed as little as
possible in order to minimise redistribution of drugs particles.
2)The analysis of counting machines is undertaken
by running pieces of paper (which have been shown to be clean)
through the counting machine.
Vacuum Cleaners
1)The dust in vacuum cleaner bags can be analysed for
traces of drugs, and this can be useful to help identify a
link with drugs. The major advantages of vacuum cleaner bags are that the
suspect may have taken the samples, and that the samples have been taken
over a longer period of time.
2)Vacuum cleaner bags should again be disturbed as little
as possible in order to minimise redistribution of drugs particles.
Hand Swabs
1)Hand swabs should be taken from a suspect as
soon as possible to try and minimise the loss of drugs traces from
the hands by abrasion. The swabs can be either dry swabs or moist
swabs.
2)Untouched swabs, and swabs with just water on
them (in the case of moist swabs) should be submitted for analysis
in order to show that the swabs themselves and the water used are
free from contamination.
Papers
1)Any papers (other than banknotes) can be
analysed for traces of drugs in the same way as banknotes. Examples
of the types of papers that can be analysed include diaries, alleged
price lists, any documentation, or any papers that may have come
into contact with drugs.
2)Paper exhibits should be treated in the same
way as banknotes.
Other Items
1)Many other items can be analysed for the
presence of drugs traces. Items can either be submitted directly for
analysis, or can be sampled remotely. The samples taken can then be
submitted for analysis.
2)Examples of the types of items that can be
submitted for analysis are remote controls, swabs from television
screens/ computer monitors, computer keyboards, carpets, weighing
scales, and any other dust samples.
3)These items can either be submitted directly to
the laboratory for analysis, or can be sampled using lint brushes
(for carpets), cotton swabs (for dust samples, monitors, scales) or
toothpicks (for keyboards and remote controls).
Document Reference : MSA4648JBL
Version No. 2
Date : 30/01/2004
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| Press Release June 2007 : UKAS 17025
Accreditation
Mass Spec Analytical Ltd achieves UKAS 17025 Accreditation
in areas of Drugs on Money, Packaging, Fuel Analysis and
Alcohol in Blood and Urine Analysis :
see Press Release
Press Release April 2007 from Applied Biosystems
Mass Spec Analytical advances forensic science
through the development of innovative technology
- see Press
Release
Mass Spec Analytical
matching of packaging
material/tape published
in The Analyst journal
http://www.msaltd.co.uk/papers.htm
News Articles:
Mass Spec ensures crime doesn't pay
http://www.rsc.org/chemistryworld/News/2005/July/06070502.asp |

Mass Spec Analytical's Forensic Scientist /
Analytical Chemist team develop a reader
which analyses 1000 tickets per hour to detect
multiple explosives simultaneously |

Our Scentinel® multi-purpose
mobile Mass spectrometer
has
been developed with
MDS Sciex Inc. and
J.S. Chinn P.E. Ltd.
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